Silk Road forums

Market => Product requests => Topic started by: jacque on September 16, 2012, 01:11 am

Title: I need Hydrazine
Post by: jacque on September 16, 2012, 01:11 am
I am trying to perform a Huang-Minglon modification wolff-kishner reduction. Let me know if anyone has any hydrazine, KOH, or ethylene glycol. I can get the other stuff by the hydrazine is the big thing.
Thanks
Title: Re: I need Hydrazine
Post by: darryl1975 on September 16, 2012, 05:29 am
Friend, you need di or tri ethylene glycol. You can use any alkali hydroxide, doesn't have to be KOH. Hydrazine hydrate is kind of hazardous to ship, buy a couple kilos of the sulphate, freebase it and make the hydrate yourself. It should all be otc. None of those are list one or two chemicals, did you try google or ebay? LOL I know where you're headed with this and there are easier ways to p2p. I assume you're doing this because you already have a good supply of cinnemaldehyde?
Title: Re: I need Hydrazine
Post by: jacque on September 16, 2012, 08:01 am
I am not headed to p2p but good guess. I do not need di or tri ethylene glycol i need ethane-1,2-diol also know as ethylene glycol.
 thank you for the response.
Title: Re: I need Hydrazine
Post by: darryl1975 on September 17, 2012, 04:01 am
I apologize for assuming then. I thought you were headed to p2p by means of the propenylbenzene intermediate. Mind sharing what you're making then? If it isn't too personal that is. I'm not sure what other use a wolff-kishner reduction would have in the way of clandestine chemistry. I'm assuming it was caldestine, again, I suppose that might be a mistake, lol. I think the sulfate will be your easiest way to the hydrate, unless you want to horse around with gelatin and try making it yourself.
Title: Re: I need Hydrazine
Post by: jacque on September 17, 2012, 04:48 am
No need to apologize. Do you know where I could get some hydrazine sulfate under the radar? That would work very well and I can get KOH really easily. The last thing would be ethylene glycol. I was thinking that the ethylene glycol could be interchanged with DMSO. That would increase the rate significantly.
Title: Re: I need Hydrazine
Post by: darryl1975 on September 17, 2012, 05:23 am
Sure do. You get the best prices when you get 25kg or more at a time. It's usually 25kg containers actually. I'll send you a pm with details in a couple minutes.