Silk Road forums
Market => Rumor mill => Topic started by: calcium on December 05, 2011, 07:11 am
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If you have done OBJECTIVE testing of a vendor's drugs, please post your results here. (Include relevant details, eg test method, % content breakdown, Marquis reagent reaction, etc.)
Objective means things like:
- Bluelight's test kit for MDMA - http://wiki.bluelight.ru/index.php/Ecstacy_Testing_Kits
- chemical analysis of % THC content by weight
- mass spec (for the hardcore chemists in the audience)
- etc
Please don't comment if your results are just from sampling it yourself, no matter how experienced you are. (You might eg have consistently had street "MDMA" that was actually 50% methamphetamine, so there's no way to know whether your experience is a good measure.)
If your tests are of your own supply, go ahead and post, but be upfront about it and expect a little skepticism. ;-)
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I have tested vortexmilkman's meth and it came back positive. I tested whatever the fuck I got from timetraveler and it wasn't meth. Used Meth-X test kits. Unfortunately I don't have the equipment to do purity testing.
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I have tested vortexmilkman's meth and it came back positive.
What reagent does Meth-X have? "Positive" on this test (I'm guessing without knowing what it is) probably means "primarily contains some form of amphetamine". Other kinds of amphetamines (eg MDMA, ephedrine, STP) could false positive this test.
Still, good sign, thanks for the review.
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I have tested Blaatz0r's speed, with all ez test reagents. Mandelin and marquis indeed showed that it is speed like substance. Simons nothing so no meth. But robadopes should be red and actually nothing happened. Although i believe my kit isnt good anymore since i keep it out of fridge and i may have contaminated it.
I have also tested Streetpharmacies and AAkoven speed. As i can remember they were amph according to ez test
I totally like this thread. I am happy to see more people sending tests results.
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Got a pretty standard routine for new substances- marquis, then melting point, then an MS in methanol. For MDMA a recrystallization from IPA/ ether, wash crystals with cold ether and compare weight, record melting point of recrystallized material and test again with marquis.
Mitanox, Ivory: MDMA >80% pure. Koekwous23's was above 90% but he no longer sells. Aakoven's orange batch is about 85%.
Sunshine's 2C-B is 100% pure.
Testing DrAmsterdam's MDMA today, will post results.
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nice!
DrAmsterdam is close to 95% pure! the crude looked like there was a little MDP2Pol but not much else, slight spicy smell when I opened the baggie but that seemed to disappear overnight when left in a beaker. 1050 mg of the material from silkroad dissolved in 3.5 mL hot IPA, cooled slowly over 4 hours then freezer for 1 hour. Washed with 5 mL cold acetone, then 2x 5 mL cold ether and the precipitate filtered and placed under vacuum. Gave 960 mg blisteringly white snowflakes, one peak by electrospray ms, sharp 153C melting point, marquis straight to black. cleanest stuff ive come across so far.
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Wowzers - I have to compliment you on your technique. Now that's doing it for real. ;-)
If you're able, photo/video (properly scrubbed of course) of stages of the process would be nice, so that we could all see what you're talking about. It'd be a public service.
For that matter, what about submitting samples to known good agencies like DanceSafe for external confirmation?
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cheers :D Next time I buy some MDMA I'll do a photo-tutorial, I'm saving up to buy a 10g pack so have quite a bit of material to work with. I'll change the tutorial a bit to use materials which anyone can get hold of (ie- no ether). I'll need to read up about cleaning images, I took a photo of the cleaned crystals but my DSLR leaves some VERY revealing EXIF data (lens serial numbers etc).
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materials which anyone can get hold of (ie- no ether)
You can get bottles of lab-grade ether on ebay. It's useful for eg making extractions from certain seeds.
I'll need to read up about cleaning images, I took a photo of the cleaned crystals but my DSLR leaves some VERY revealing EXIF data (lens serial numbers etc).
Definitely scrub your stuff before posting.
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I'm trying to find out what Meth-X uses and what false positives there are but I don't see this information in the description. The test substance came in a plastic tube with two glass ampules to break and mix. The substance to be tested was rubbed on a piece of paper and then a couple drops of reagent were applied to the test paper. It turns blue if meth or ecstasy are detected. I wouldn't use it to test ecstasy since it can be cut with meth, but it's extremely unlikely for meth to be cut with ecstasy.
Excellent work with the purity testing. I wish I had the knowledge and materials for detailed analysis. I'd especially be interested in testing H for purity since it varies so wildly and is much easier to OD on than X or crystal.
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Its probably Simon's Reagent. The paper is probably impregnated with sodium nitroprusside, then the 2 ampules contain something like sodium carbonate solution and acetone. meth and mdma turn blue. Marquis reagent (19:1 sulfuric acid/ 37% aqueous formaldehyde) will discriminate between the two. It's rare in Europe to see ecstasy contaminated with meth, seems to be more of a US/ Aus problem.
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Just another objective test for DRAmsterdam molly crystal. Dancesafe kit is approx 8 months old (probably not properly stored). I haven't sampled the goods yet.
Results came out beautifully:
Mecke: Very quick green to blue.
Marquis: Purple - Black quickly, slight smoke
Simon's: Slower reaction to cobalt blue, about 10 sec.
Results here: http://i.imgur.com/cGJ2R.jpg
Edit: Order received January 2012 USA