Silk Road forums
Market => Product offers => Topic started by: ThreeKings on September 23, 2013, 04:51 pm
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Good day Ladies and Gentleman
Maybe some serious chemists would be interested in
MDA precursor
N-[1-(1,3-benzodioxol-5-yl)propan-2-yl]acetamide
Chemnet link:
http://www.chemnet.com/cas/en/36209-71-9/N-[1-(1,3-benzodioxol-5-yl)propan-2-yl]acetamide.html **** CLEARNET WARNING ****
Some brief synthesis to gain Mda would be :
10 grams of Sodium Hydroxide in 200ml of water in a 500ml flask is added
20 grams of the AMIDE and 250 grams of Bleach. The mixture is then heated
to 80C with stirring. At about 50-60C the mixture can become white as the
carbonate forms. At 70-80C an oil seperates. (this is crude MDA). The
solution was cooled and extracted with Xylene. The solution was filtered
and the filtrate washed with xylene and the xylene portions each added
together. About 100ml of Muriatic acid was added to the xylene, shaken and
seperated. The aqueous solution was extracted with xylene and the xylene
seperated. The amine was then liberated from the aqeuous portion with
Sodium Hydroxide and worked up in the usual way to give MDA.
please write me to my SR profile - hardly checking here