Looking for Alprazolam Powder/API

Right now it looks like I'm going to go with luckyduck, but does anyone else have any other suggestions, or even comments on luckyduck? I read somewhere on this subreddit that his powder feels just like Rx Xanax, which is what I'm looking for.


Comments


[5 Points] fakes12345678:

His powder is diveredted from a pharama company before being presed into pills.

With the producer I got nothing... month + later no love leter or anything but he did give me a refund as i grabbed his $60 g sample when he first started got 1.5g just because ... not sure now that he is bigger if he will do that without tracking...

Lucky duck. I got his shit tested. 99.5% 2 seprate samples 1 by me and a NMR graph as well using a tor link if you understand using the anin link if you dont know analytical chem dont bother.


raw data:

NMR sample: (200 MHz, CDCl3) delta = 7.52-7.40 (m, 7H, Ar-H), 5.48 (d, 1H, CH2), 4.07 (d, 1H, CH2), 2.61 (s, 3H, CH3), 1.88 (s, 2H, H2O) ppm.

literature (http://www.drugbank.ca/drugs/DB00404): (400 MHz, CDCl3) delta = 7.83-7.38 (m, 8H, Ar-H), 5.27 (d, 1H, CH2), 4.23 (d, 1H, CH2), 2.66 (s, 3H, CH3) ppm.

Thermal analysis m.p. 225 C literature: 228.5-229 C

EA Calculated C 62.48 %, N 17.15 %, H 4.63 % Found C 62.88 %, N 17.20 %, H 4.47 %

https://anonfiles.com/file/0c9c5337a8ec7b9cc4311a817e5ba5aa

Here is some icing on the cake- some test results came back. I'm am very

pleased with them and I'm sure you will be too:

results are all in, double checked It is INDEED almost analytically pure

99.5 alprazolam monohydrate. How I got to the conclusion:

  1. 1H-NMR: (just a recap of what I already wrote) Spectrum shows clearly shows one methyl group (3H signal upfield) and 2 aliphatic C-H signals in the middle (corresponding to the CH2 group on the big, non-aromatic ring. they are split into two signals for reason of asymmetry.). The aromatic signals are complicated and hard to analyze, we could only find 7 out of the expected 8 hydrogen atoms. This had me become suspicious whether the sample wasn't a cheap, substituted derivative of the Alpra. But I kept in mind the possibility of not fully accurate measuring (can happen for aromatics as well as OH and NH2). So I postponed final judgment for now. Apart from those clearly alprazolam-related signals, there were traces of silicone grease (meaningless, extremely small amounts, non-toxic) and 1 mol H2O as a clear signal. So even though alprazolam is a hydrophobic substance, the sample exists as alprazolam monohydrate. No big deal however, this amounts to about only > .5 % less active compound by weight. Heck, we`ve already seen (otherwise pure) oxycodone TRIhydrate before, which should have been the anhydrous form... Chemistry, man, whatever. Ok, but the troublesome 7/8 aromatic H atoms warranted further testing:

  2. Thermal analysis: a very slight endothermic event at 104 ?C which I interpret as boiling off of the H2O. Then a large endothermic event at 225 ?C, then nothing more until 450 ?C (where the measurement terminated). The 225 ?C event is merely a few degrees below the literature figure for the melting point. So yeah, that's just about perfect.

  3. Elemental analysis: C, H and N content almost spot on for those calculated for alprazolam monohydrate. No room for any additional Br or Cl on any ring whatsoever. No more to say here.

Had this been a novel compound synthesized by a research group, there would be no delay in publishing these results immediately (although probably generously rounding up for the NMR integral, these cheaters). The technical details are further down.


Technical information/raw data:

NMR sample: (200 MHz, CDCl3) delta = 7.52-7.40 (m, 7H, Ar-H), 5.48 (d, 1H, CH2), 4.07 (d, 1H, CH2), 2.61 (s, 3H, CH3), 1.88 (s, 2H, H2O) ppm.

literature (http://www.drugbank.ca/drugs/DB00404): (400 MHz, CDCl3) delta = 7.83-7.38 (m, 8H, Ar-H), 5.27 (d, 1H, CH2), 4.23 (d, 1H, CH2), 2.66 (s, 3H, CH3) ppm.

Thermal analysis m.p. 225 ?C literature: 228.5-229 ?C (http://www.drugbank.ca/drugs/DB00404)

EA Calculated C 62.48 %, N 17.15 %, H 4.63 % Found C 62.88 %, N 17.20 %, H 4.47 %


[3 Points] sorudesandstorm:

A good buddy of mine ordered 1g via reg mail from theproducer. Due to late ass fucking canada shits, he gave my friend 3.5g instead! Also with a cherry bonus of top of tracking


[3 Points] TheOpiateKing:

TheProducer is your man.


[2 Points] gotothepoppies3:

Maybe you read my comment but LD/LS has awesome powder. I've gotten about 5g altogether over 3 orders and just put in another 2g order yesterday. Never anything but fast shipping and great quality.

I actually don't think that I've ever even messaged with him/her/them, I just place the order finalize when I see it marked shipped and stay in good quality powder. I haven't even weighed since the second order. First was 1g and weighed 1200mg or so and the second was 2g and weighed 2200mg+.

I will say dilution in pg is more difficult than I'm used to. In Everclear or the 192 proof Polish "Polmos Spirytus" line of liquors it's unbelievably easy. 2g in 200ml takes around 30 seconds of shaking to dilute completely.


[2 Points] fakes12345678:

oh and his turn in atest for 5g became 10.5g. he will no longer use EC or dancesafe for the promotion. must use NMR machines that that 2-3 weeks to test only.


[1 Points] aboutthednm:

Theproducer has good stuff